Ex parte MASUKO et al. - Page 3




                                                                                       Page 3              


                                               THE CLAIMS                                                  
            Claims 22 and 43 are illustrative of appellants’ invention and are reproduced                  
            below.                                                                                         
            22.  A method of producing a coating fluid to be applied to the                                
            surfaces     of parts of a polymerizing apparatus that will come into contact with             
            vinyl                                                                                          
                  monomer which is to be polymerized in an aqueous medium or subjected to                  
                  mass-polymerization so that the produced vinyl chloride polymer is prevented             
            from adhering to said surfaces, which method comprises modifying an initial                    
            condensate obtained by condensing at least one phenol and at least one aldehyde in             
            the          presence of a basic catalyst with a modifier to produce a modified                
            phenolic resin,    diluting the obtained alkaline liquid with water so that the                
            concentration of said    reaction product has a prescribed value, adding the diluted           
            liquid to an acid to adjust the pH thereby depositing said modified phenolic resin, and        
            separating the     deposited modified phenolic resin and dissolving said modified              
            phenolic resin in an     organic solvent or an aqueous alkali solution having a pH             
            for dissolving said modified    phenolic resin.                                                
                        43.  A method of preventing scale from adhering to the inner wall                 
            surfaces     of a polymerization tank and the like used in the polymerization of vinyl         
            chloride     monomers, comprising:                                                             
                         preparing an aqueous coating fluid which is an aqueous alkali solution            
                         containing a modified phenolic resin in an amount of 0.1 to 10.0 wt. %            
            and having a pH adjusted with an acid to a pH of 0.2 to 4.0 higher than the pH at              
            which the    modified phenolic resin deposits at ambient temperature; and                      
                         applying the coating fluid to the surfaces wherein the temperature of             
            the surfaces has been previously elevated to 40EC or over and wherein the                      
            modified     phenolic resin is deposited from the aqueous coating fluid and adhered            
            to the       surfaces.                                                                         
















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