Ex parte ROCHAT et al. - Page 6




          Appeal No. 95-4721                                                          
          Application No. 08/128,332                                                  


          probative value of the declaration is not commensurate in                   
          scope with the degree of protection sought by the appealed                  
          claims.  In re Grasselli,                                                   
          713 F.2d 731, 743, 218 USPQ 769, 778 (Fed. Cir. 1983); In re                
          Clemens, 622 F.2d 1029, 1036, 206 USPQ 289, 296 (CCPA 1980).                
          Example 1 of the specification that is reported in the                      
          declaration uses a temperature of 180EC which is considerably               
          above the lower limit of the claimed range of 100EC.  While                 
          appellants contend at page 7 of their principal Brief that                  
          180EC is representative of the claimed range of 100E-220EC, no              
          factual basis is offered for this conclusion.  If, as                       
          appellants argue, it is unexpected that the claimed amination               
          of an aryl halide gives high yields at a temperature as low as              
          180EC, it is reasonable to require appellants to demonstrate                
          that a similar unexpected yield would result at a temperature               
          that is considerably lower than 180EC, viz., at the claimed                 
          100EC.  In our view, the single temperature used in the                     
          declaration does not establish unexpected results for the                   
          claimed range which substantially coincides with the preferred              
          temperature range disclosed by Dix.  In re Greenfield, 571                  
          F.2d 1185, 1188,                                                            

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