Ex parte SUCIU et al. - Page 2




               Appeal No. 95-5092                                                                                                 
               Application 08/032,581                                                                                             


                      1.  A process of reducing hexavalent chromium to trivalent chromium and                                     
                      precipitating the trivalent chromium from a waste water stream to form a                                    
                      sludge for disposal, said process comprising the steps of:                                                  
                              (a)  adding soluble sulfide ion to said stream in a ratio of sulfide ion to                         
                              hexavalent chromium of from about 0.7 to 2.5;                                                       
                              (b)  adding soluble ferrous ion to said stream in a ratio of ferrous ion                            
                              to hexavalent chromium of from about 0.5 to 5.0.;                                                   
                              (c)  thereafter adjusting pH of said stream to about 7.2 to 8.4;                                    
                              (d)  adding a flocculating polymer to said stream to promote                                        
                              formation of a floc comprising precipitated trivalent chromium;                                     
                              (e)  forming a sludge bed comprising said precipitated trivalent                                    
                              chromium; and                                                                                       
                              (f)   thereafter filtering the floc from said stream using said sludge bed                          
                              containing said precipitated trivalent chromium.                                                    
                      The examiner relies upon the following references as evidence of obviousness:                               
                      Senda et al.           4,362,629                      Dec. 07, 1982                                         
                      Aldrich                4,705,639                      Nov. 10, 1987                                         
                      Schlauch et al.  (Schlauch) , "Treatment of Metal Finishing Wastes by Sulfide                               
                      Precipitation," Report No. EPA-600/2-77-049 (Feb. 1977).                                                    
                      Appellants' claimed invention is directed to a method of treating waste water to                            
               reduce the hexavalent chromium therein to trivalent chromium.  The method involves                                 
               adding soluble sulfide ion and soluble ferrous ion in the recited amounts to the waste water                       
               stream and thereafter adjusting the pH of the stream to about 7.2 to 8.4.                                          


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