Appeal No. 95-5092 Application 08/032,581 less than the presently claimed lower limit of 0.5 (50%). Furthermore, at Col. 6, lines 36 et seq., Aldrich teaches that the logical step in order to avoid an excess of sludge would be to eliminate the iron from the treatment process, but in such cases, undesir-able H S gas 2 would be produced. Therefore, Aldrich teaches that using limited ferrous ion dosages of 10-20% would inhibit the production of H S gas as well as produce a 60 to 70% reduction 2 in sludge. Accordingly, taking into consideration the entirety of the Aldrich disclosure, we fail to find any teaching or suggestion or motivation for one of ordinary skill in the art to perform the Aldrich process by using the claimed amounts of ferrous ion. While the examiner states at page 4 of the final rejection that the claimed ratio of ferrous ions "would have been an obvious matter of process optimization to one skilled in the art", it has been generally held that it is not a matter of prima facie obviousness for one of ordinary skill in the art to optimize a value outside the operable range disclosed by the prior art. In re Sebek, 465 F.2d 904, 907, 175 USPQ 93, 95 (CCPA 1972). The examiner also states at page 4 of the answer that "[a]ppellants have not presented sufficient factual comparative evidence to show that these amounts are required for the successful reduction of hexavalent chromium to trivalent chromium and the precipitation of trivalent chromium at the pH range recited in the instant claims." 4Page: Previous 1 2 3 4 5 6 NextLast modified: November 3, 2007