Appeal No. 1997-1461 Application 08/388,915 stream. Claim 1 is illustrative and reads as follows: 1. Method for recovering particulate silicon from a liquid by-product stream, the method comprising: (A) substantially separately a liquid stream comprising particulate silicon, a metal salt, and a high-boiling silicon containing compound having a boiling point higher than the sublimation temperature of the metal salt, into a liquid component and a particulate component where the particulate component comprises the particulate silicon, the metal salt, and residual high-boiling silicon containing compound; (B) washing the particulate component with a solvent having a boiling point lower than the sublimation temperature of the metal salt, thereby essentially separating the residual high-boiling silicon containing compound from the particulate component, and (C) recovering the particulate component by spray drying at a temperature lower than the sublimation temperature of the metal salt. The references relied upon by the examiner are: Kotval et al. (Kotval) 4,195,067 Mar. 25, 1980 Ritzer et al. (Ritzer) 4,892,694 Jan. 9, 1990 Burgie et al. (Burgie) 5,118,486 Jun. 2, 1992 Chadwick et al. (Chadwick) 5,326,896 Jul. 5, 1994 Claims 1, 2, 4, 5 and 9 stand rejected under 35 U.S.C. § 103 as being unpatentable over Chadwick and appellant’s 2Page: Previous 1 2 3 4 5 6 7 8 9 NextLast modified: November 3, 2007