Ex Parte PARE - Page 4




                 F 16. ParC s claims I and 10 are representative of the parties' subject matter as claimed by Pare                                                     
                          (paragraphing added):                                                                                                                        
                           I . In a method for the microwave extraction                                                                                                
                                              of at least one natural product                                                                                          
                                              from a biological material,                                                                                              
                                    said method consisting in:                                                                                                         
                                              placing said biological material in an enclosure                                                                         
                                                       without any solvent,                                                                                            
                                              making said biological material present in said enclosure undergo                                                        
                                                       microwave irradiation                                                                                           
                                                       in order to prompt the evaporation of at least a part of                                                        
                                                                 the water contained in said biological                                                                
                                                                 material,                                                                                             
                                                       so as to enable the release of at least a part of said natural                                                  
                                                       product,                                                                                                        
                                              separating the residual biological material from the extracted natural                                                   
                                                       product,                                                                                                        
                                    the improvement wherein said method includes the steps of                                                                          
                                              cyclically intermittently applying reduced pressure                                                                      
                                                       within said enclosure                                                                                           
                                                       during said step for the application of microwaves,                                                             
                                              heating said enclosure                                                                                                   
                                                       during at least the essential part of said step for the                                                         
                                                                 application of microwaves,                                                                            
                                              the combination of said steps for the application of the microwaves,                                                     
                                                       the application of reduced pressure within the enclosure and                                                    
                                                       the heating of the enclosure permitting the volatilization of                                                   
                                                       said natural product from said biological material.                                                             
                           10. A method of microwave extraction                                                                                                        
                                              of at least a natural product                                                                                            
                                              from a biological material containing volatilizable components,                                                          
                                    comprising                                                                                                                         
                                              providing a matrix of biological material                                                                                
                                                       having volatilizable components dispersed therein,                                                              
                                              treating said matrix with microwave energy                                                                               
                                                       to effect volatilization of at least one of the volatilizable                                                   
                                                                 components from the biological material,                                                              
                                              cyclically intermittently applying reduced pressure during the                                                           
                                                       microwave treatment, and                                                                                        
                                              separating at least one volatilized component                                                                            

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