Appeal 2007-1938 Application 10/050,437 electrical properties of an aerogel with the strength of an RVC (Specification ¶ 4). [3] According to the specification, "[t]he structure of the final carbon product of this invention consists of a matrix of porous carbon aerogel, reinforced by solid carbon struts, all in intimate contact so that the strength of the composite is maximized" (Specification ¶ 11). [4] Further according to the specification, the composite is made by infiltration of an organic gel precursor into a pre- formed organic polymer foam, where it gels. The gel composite is then dried by any method that minimizes shrinkage of composite material. Whereafter, the dried gel composite is heated in a furnace to pyrolyze the composite, reducing it to a glassy carbon form. [Specification ¶ 11.] [5] The organic gel precursor may be an aqueous solution comprising resorcinol, formaldehyde and sodium carbonate (Specification ¶ 14). [6] The organic polymer foam may comprise a phenol-formaldehyde resin (Specification ¶ 14). [7] Gelling may occur at a 80oC for 30 to 180 minutes (Specification ¶ 14). [8] Drying may occur by evaporation for 12 to 48 hours or by supercritical drying after fluid exchange with liquid carbon dioxide (Specification ¶ 14) [9] Pyrolyis may be at a temperature of 700 to 1100oC for 8 to 12 hours (Specification ¶ 14). [10] Pyrolysis is said to simultaneously decompose both the organic polymers "so that the shrinkage of each occurs in a manner that 4Page: Previous 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Next
Last modified: September 9, 2013