Appeal 2007-2124 Application 10/175,515 6. The basic solution is combined with an acid solution containing zirconyl ion to precipitate the zirconyl tungstate matrix (Ehrhardt, col. 3, ll. 24-27 and 60-68). 7. “It is preferable to slowly add the basic tungsten solution to the acid solution . . . to promote formation of zirconyl tungstate. This is because of the tendency of the zirconyl cation to form zirconium hydroxide” which is undesirable (Ehrhardt, col. 4, ll. 5-12). 8. After the zirconyl tungstate matrix is precipitated, the pH of the slurry comprising the matrix is adjusted to from 5 to 7 using a base such as sodium hydroxide to prevent the zirconyl tungstate from re-dissolving (Ehrhardt, col. 4, ll. 19-23). 9. “Any zirconium hydroxide which forms from the excess zirconyl cation used as described above, may precipitate when the slurry is adjusted to a basic pH. This precipitate may remain associated with the matrix and adsorb any solubilized tungsten released from the matrix which would otherwise contaminate the eluate” (Ehrhardt, col. 4, ll. 23-29). 10. The matrix material may be transferred to an empty container, such as a glass column used in standard chromatography, for eluting and harvesting the daughter compound Re-188 (Ehrhardt, col. 4, ll. 40-47). DISCUSSION The dispute in this appeal turns on the proper interpretation of the phrase “inorganic layered hydroxide.” The Examiner contends that Ehrhardt teaches a tungsten compound which contains hydroxide, meeting the limitation in claim 1 of an “inorganic layered hydroxide” (Answer 3-4). Appellants assert that the Examiner improperly interprets the claimed 5Page: Previous 1 2 3 4 5 6 7 8 Next
Last modified: September 9, 2013