Appeal No. 1996-3017 Application No. 08/851,810 presented no objective evidence that adjusting the reaction mixture to an alkaline pH produces an unexpected result. We now turn to the examiner's rejection of claims 6-10, 13, 19 and 20 under 35 U.S.C. § 103. Independent claim 6 calls for preparing alkyl-pyrazines by "heating, refluxing and subliming" an aqueous medium containing ammonium ions and an acyloin compound as reactants. While the primary references do not disclose sublimation, appellant does not dispute the examiner's factual determination that Evans discloses the isolation of alkyl-pyrazines by a sublimation technique. Since Weissberger evidences that sublimation was a well-known technique for isolating volatile compounds, in general, and Evans evidences that it was known in the art to employ sublimation to isolate alkyl-pyrazines, we find no error in the examiner's conclusion that it would have been obvious for one of ordinary skill in the art to employ such a well-known separation technique to isolate the alkyl-pyrazines produced by the methods of the primary references. In effect, our analysis is much the same as that discussed above with respect to the rejection of claim 2. -8-Page: Previous 1 2 3 4 5 6 7 8 9 10 11 12 NextLast modified: November 3, 2007