Appeal No. 1996-3470 Application 08/313,179 aluminum. The claimed process requires that the metal surface is contacted with a phosphating solution containing zinc ions; copper ions; phosphate ions; manganese ions; and importantly, at least one member selected from the group consisting of hydroxylamine salts, hydroxylamine complexes and hydroxylamine. Such a phosphating solution provides a crystalline coating on the metal surfaces containing an edge length of the phosphate crystals of from 0.5 to 10 microns. The coating produced by the process of the claimed invention is said to provide a firm lacquer adhesion and excellent corrosion protection to the metal surfaces treated. As evidence of obviousness of the claimed invention, the examiner relies on the combined disclosures of Gehmecker, Kramer, and Müller. Similar to appellants' claimed process, Gehmecker discloses a process for the production of nickel-free phosphate coatings (column 2, lines 48-54) on steel, galvanized steel, and aluminum surfaces which phosphate coatings provide advantageous corrosion protection for the metal surfaces. Additionally, Gehmecker's phosphate coatings are advantageously used to prepare the metal surfaces for a subsequent lacquer coating. See column 4, lines 57 through 64 of the reference. Gehmecker's phosphating solution, which is substantially free of nickel, contains zinc 3Page: Previous 1 2 3 4 5 6 7 8 9 10 NextLast modified: November 3, 2007