Ex parte ROLAND et al. - Page 7



          Appeal No. 1996-3470                                                        
          Application 08/313,179                                                      



          prior art compositions.  In addition, appellants allege that they           
          have unexpectedly discovered that the corrosion resistance of a             
          zinc surface which has been phosphated according to the process             
          of the present invention with a phosphate bath which is free of             
          both nitrite and nitrate is superior to the corrosion resistance            
          of coatings produced from the phosphating solutions containing              
          nitrite ions as described in the prior art references.  However,            
          we observe that Gehmecker describes the phosphate coatings                  
          provided by his process as providing advantageous protection                
          against corrosion, and we further observe that appellants have              
          made no comparative study with respect to the corrosion                     
          resistance of coatings produced from the specific phosphating               
          solutions utilized by Gehmecker, particularly, Gehmecker's                  
          working Example 12 which apparently contains no nitrite or                  
          nitrate ions.  We also observe that Gehmecker indicates that                
          preferred oxidizers include chlorates, bromates and peroxy                  
          compounds which oxidizers may be used alone and not necessarily             
          in combination with nitrate or nitrite oxidizers.  See Gehmecker            
          at column 3, lines 52 through 65.  Moreover, although appellants            
          contend that comparative Example 2 in the specification                     
          (specification, pages 12 through 16) illustrates the improvement            
          of a coating formed over that obtained by using a nickel                    

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