Interference No. 104,101
Page 12
confirm” that he had prepared a compound depicted on page 266 of his notebook, which has the
following structure:
(EX 1152, ¶ 36). Laboratory notebook page 266 has the number “311583" written next to the
above depicted structure.
F25. Mr. Cullinan has failed to explain how the “proton NMR analysis and the elemental
analysis helped to confirm” that he had made the compound depicted on page 266 of his
notebook. Specifically, Mr. Cullinan has failed direct our attention to the underlying proton
NMR data and explain how that test data would support a conclusion that he had prepared the
identified structure.
F26. The March 17 portion of Mr. Cullinan’s laboratory notebook page 266 depicts the
chemical structure Mr. Cullinan is said to have prepared and contains the notation “NMR: O.K.”1
(EX 1201, Bates No. 3013). The notebook page fails to identify the underlying data for the
proton NMR analysis.
1We understand “NMR” to mean nuclear magnetic resonance.
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